Method of making a silicon nitride part

Plastic and nonmetallic article shaping or treating: processes – Including step of generating heat by friction

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264 65, 264 81, 264 86, 264325, C04B 3558

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043104770

ABSTRACT:
A method of making a silicon nitride part is disclosed. In this method an article of silicon nitride is first made which has a density less than the theoretical density of silicon nitride. This article also contains a densification aid. The entire surface area of this article is coated with a thin silicon nitride skin which is gas impervious. The so coated article is heated to a temperature for a time sufficient so that some of the densification aid may diffuse into the silicon nitride skin. The so treated article is then subjected to a pressure sufficiently high, for a time sufficiently long and at a temperature which permits the silicon nitride article and skin thereon to be compacted to increase the density of the article to a density greater than it originally had and to form the silicon nitride skin about the article so that the skin becomes an integral of the finished part.

REFERENCES:
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patent: 3455682 (1969-07-01), Barbaras
patent: 3469976 (1969-09-01), Iler et al.
patent: 3819787 (1974-06-01), Coe
patent: 3854189 (1974-12-01), Ezis
patent: 3887411 (1975-07-01), Goodyear et al.
Airey, Pyrolytic Silicon Nitride Coatings, Proc. Brit. Cer. Soc., No. 22, Jun. 1973, pp. 305-320.
Gazza, Hot Pressed Si.sub.3 N.sub.4 , J. Am. Cer. Soc., vol. 56, No. 12, p. 662.

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