Apparatus for catalyst analysis

Chemical apparatus and process disinfecting – deodorizing – preser – Analyzer – structured indicator – or manipulative laboratory... – Means for analyzing liquid or solid sample

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422 78, 422 80, 422 50, 436 37, 436155, 436159, G01N 3110, G01N 3112, G01N 2172

Patent

active

050394894

ABSTRACT:
An improvement in an apparatus for carrying out chemical reactions is disclosed. The apparatus includes a housing defining a vacuum chamber, with a reactor located within the vacuum chamber. The improvement comprises a device disposed within the housing having a high-pressure outlet tube for engagement with the reactor, a bypass for placing the high-pressure outlet tube in fluid communication with the outside of the vacuum chamber, an orifice for placing the high-pressure outlet tube in fluid communication with the vacuum chamber and at least one valve for selectively opening or closing the bypass and the orifice. The device may be engaged and disengaged with the reactor by a manual shaft and gear arrangement for operating the reactor at higher pressures relative to the normal vacuum operation.

REFERENCES:
patent: 3223492 (1965-12-01), Geitz
patent: 4626412 (1986-12-01), Ebner et al.
patent: 4677244 (1987-06-01), Hachmuth et al.
Machiels, Development of a Pulse Reactor with On-Line MS Analysis to Study the Oxidation of Methane, American Chemical Society, 1982.

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