Preparation of RDX

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07D25154

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039377032

ABSTRACT:
RDX is produced by reacting formaldehyde and an alkyl nitrile RCN, wherein is an alkyl group of 1 to 3 carbon atoms, in the absence of added solvents, to form a 1,3,5-triacylhexahydro-s-triazine and subjecting the latter, without separation thereof from the reaction mixture, to nitrolysis by contact with concentrated nitric acid to form RDX.

REFERENCES:
patent: 2559835 (1951-07-01), Zerner et al.
patent: 2568620 (1951-09-01), Gresham et al.
patent: 3178430 (1965-04-01), Thatcher

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