Method for making aromatic bis(ether dicarboxylic acid)

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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2603434, 260516, C07C 5100

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active

040051340

ABSTRACT:
A method is provided for making aromatic bis(ether dicarboxylic acid) useful for making high performance injection moldable polyetherimides. An aromatic bis(ether N-organo phthalimide) is hydrolyzed directly to the corresponding tetra-acid by heating the aromatic bis(ehter N-organo phthalimide) in a closed system in the presence of acetic acid, water, and a mineral acid.

REFERENCES:
patent: 3247208 (1966-04-01), Schenker
patent: 3875208 (1975-04-01), Cohen et al.
patent: 3879428 (1975-04-01), Heath et al.
patent: 3903101 (1975-09-01), Yoshida et al.
Weygand, "Prep. Org. Chem.," p. 450, John Wiley & Sons (1972).
Moller, "Chem. of Org. Comp.," 3rd. Edition, Edition, p. 604, Saunders (1965).

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