Bonded organo-pellicular packings for chromatographic columns

Gas separation – Means within gas stream for conducting concentrate to collector

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55386, 252428, 252429R, 252430, 252441, 568750, 568758, B01D 1508, B01J 3102

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active

041993306

ABSTRACT:
Highly effective chromatographic column packings are prepared by reacting hydroxyl groups on a silica surface with SiCl.sub.4 and then reacting the chlorosilylated surface with a polyglycol or polymeric glycol ester in a slurry reaction. Residual chlorosilane groups on the reacted surface are neutralized by reaction with methanol or other lower alkanol. The resulting modified silica has a bonded, essentially monomolecular organic surface film which provides thermal stability, uniform efficiency, and rapid analysis when the material is used as a column packing in gas-liquid chromatography.

REFERENCES:
patent: 3417028 (1968-12-01), Montgomery et al.
patent: 3664967 (1972-05-01), Stehl
patent: 3722181 (1973-03-01), Kirkland
patent: 3817931 (1974-06-01), Brooks et al.
Journal of Chromotography, 135, pp. 261-272 (1977), by Sadao Mori.
Journal of Chromotographic Science, vol. 12, pp. 161-172 (4/1974), by Halasz et al.
Journal Chromotogr. Sci.; 8, 309 (1970), Kirkland.
Journal Chromotogr. Sci.; 9, 206 (1971), Kirkland.
Journal Chromotogr. Sci.; 11, 120-128 (1973), Locke.
Journal Chromotogr. Sci.; 12, 337-343 (1974), De Stefano et al.
Chromatographia; 8 (12), 661-668 (1975), Kirkland.
Anal. Chem.; 44 (1), 90-92 (1972), Locke et al.

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