Electricity: measuring and testing – Particle precession resonance – Using a nuclear resonance spectrometer system
Patent
1989-11-01
1991-08-27
Tokar, Michael J.
Electricity: measuring and testing
Particle precession resonance
Using a nuclear resonance spectrometer system
324312, G01R 3320
Patent
active
050436643
ABSTRACT:
In order to suppress a doublet structure in a carbon spectrum due to J-coupling between carbon and hydrogen spins in compounds containing at least one CH group, a first magnetic rf field having a frequency equal to the Larmor frequency of carbon is generated, after which a second magnetic rf field having the Larmor frequency of the hydrogen in the relevant CH group is applied to the examination zone, and the spin resonance signal generated is detected. Decoupling is achieved with a reduced rf load in that a magnetic rf pulse having the duration T and the amplitude B.sub.p is generated a predetermined period of time dt after the end of excitation of the carbon, after which the amplitude of the rf field is immediately reduced to a value B.sub.c and the spin resonance signal is detected, the parameters dt, Bc and Bp being chosen so that the modulation of the spin resonance signal caused by the J-coupling is exactly eliminated.
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Slobod Jack D.
Tokar Michael J.
U.S. Philips Corp.
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