Process for preparation of 5-mercaptotetrazolyl-1-acetic acid

Details Process for preparation of 5-mercaptotetrazolyl-1-acetic acid Process for preparation of 5-mercaptotetrazolyl-1-acetic acid

1979-07-05

1983-02-22

Daus, Donald G.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

C07D25704

Patent

active

043749941

ABSTRACT:
5-Mercaptotetrazolyl-1-acetic acid is prepared by bromination with molecular bromine of tetrazolyl-1-acetic acid to produce 5-bromotetrazolyl-1-acetic acid which is then reacted with thiourea to displace the bromine and, after alkaline hydrolysis, to produce 5-mercaptotetrazolyl-1-acetic acid.

REFERENCES:
Stolle et al., Siprakt. Chem. [2] 134, pp. 282-309 (1932).
Waudell Piep. of Thiols, Ch. 4 "The Chemistry of the Thiol Group", Part I. Patai (ed), pp. 186 & 187, Wiley, N.Y., (1974).

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