Purification of chloronitrosocyclohexane dimer (CNCD)

Details Purification of chloronitrosocyclohexane dimer (CNCD) Purification of chloronitrosocyclohexane dimer (CNCD)

1975-05-28

1976-05-11

Sebastian, Leland A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260707, C07C 8102

Patent

active

039564100

ABSTRACT:
Purification of chloronitrosocyclohexane dimer (CNCD) is effected by dissolving the crude CNCD in a chlorinated aliphatic hydrocarbon or a lower aromatic hydrocarbon solvent and thereafter displacing the solvent of the solution with an aliphatic alcohol of higher boiling point. Pure CNCD crystallizes and is separated from the liquors, which retain colored matter and other impurities.

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