Method of somatotropin naturation using urea and a soluble organ

Chemistry: natural resins or derivatives; peptides or proteins; – Proteins – i.e. – more than 100 amino acid residues – Hormones – e.g. – prolactin – thymosin – growth factors – etc.

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530324, 530344, 530824, 530825, 530397, C07K 308, C07K 1504

Patent

active

051091178

ABSTRACT:
A method for the solubilization and naturation of somatotropin from refractile bodies produced by r-DNA technology wherein the refractile bodies are dissolved in an aqueous solution comprising a chaotropic agent such as urea or guanidine hydrochloride and a soluble organic alcohol such as isopropanol or benzyl alcohol. The solubilized protein is exposed to mild oxidation for a time sufficient to allow the protein to form disulfide bonds and refold to its native conformation. The presence of the alcohol suppresses the formation of somatotropin dimers and aggregates and results in higher yields of the desirable monomeric form of the protein.

REFERENCES:
patent: 4511502 (1985-04-01), Builder et al.
patent: 4652630 (1987-03-01), Bentle et al.
patent: 4694073 (1987-09-01), Bentle et al.
patent: 4731440 (1988-03-01), Bentle et al.
patent: 5023323 (1991-06-01), Ho

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