Process for the manufacture of bis-(2-cyanoethyl)-amine

Details Process for the manufacture of bis-(2-cyanoethyl)-amine Process for the manufacture of bis-(2-cyanoethyl)-amine

1976-10-20

1977-10-25

Brust, Joseph Paul

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C12000, C07C12143

Patent

active

040555860

ABSTRACT:
A process for the manufacture of bis-(2-cyanoethyl)-amine wherein gaseous ammonia is reacted with acrylonitrile having a 5-15% by weight water content in a bubble column reactor. The reaction is carried out at a temperature of about 20.degree.-80.degree. C.

REFERENCES:
patent: 1992615 (1935-02-01), Hoffmann et al.
patent: 2401429 (1946-06-01), Kung
patent: 2579580 (1951-12-01), Howk et al.
patent: 3914280 (1975-10-01), Yamakami et al.
Buc, et al.; J.A.C.S., 67(1945), pp. 92-94.
Wiedeman, et al.; J.A.C.S., 67(1945), pp. 1994-1996.

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