System and method for thermogravimetric analysis

Chemistry: analytical and immunological testing – Pyrolysis – combustion – or elevated temperature conversion – Multiple stages of heating or heating at multiple...

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422 80, 422 94, 422 98, 436155, 436160, G01N 2135, G01N 2175, G01N 2500

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048247901

ABSTRACT:
An instrument for the chemical analysis of coal and other hydrocarbons combines TGA and FT-IR principles, and utilizes helium to carry the volatiles evolved by pyrolysis of the sample into the optical cell of the FT-IR spectrometer. The connection between the TGA furnace and the optical cell is substantially direct and non-impeding to fluid flow, and the carrier gas is preheated to the same temperature as the sample, preferably using a common heating element.

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Solomon et al., Amer. Chem. Soc., vol. 31, No. 1, Preprints of Papers, Apr. 13-18, 1986, pp. 1-5.

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