Process for preparing hexanitrobibenzyl

Details Process for preparing hexanitrobibenzyl Process for preparing hexanitrobibenzyl

1979-09-26

1981-01-27

Sebastian, Leland A.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

C07C 7910

Patent

active

042477247

ABSTRACT:
2,2', 4,4', 6,6'-hexanitrobibenzyl, an intermediate compound used for mak hexanitrostilbene, is prepared by dissolving trinitrotoluene in a solvent system comprising a water-immiscible solvent and an aliphatic alcohol and then adding a metal hypochlorite solution containing a metal hydroxide to the trinitrotoluene solution to form the hexanitrobibenzyl. The compound is then separated from the reaction mixture.

REFERENCES:
Shipp et al., J. Org. Chem., vol. 31, pp. 857 to 861 (1966).

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