Process for the manufacture of low density bis-maleimide-carbon

Adhesive bonding and miscellaneous chemical manufacture – Methods – Surface bonding and/or assembly therefor

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156285, 156311, 428117, 428402, 428408, B32B 312

Patent

active

041938291

ABSTRACT:
A process for the preparation of composite laminate structures of glass cloth preimpregnated with polybismaleimide resin and adhered to a polybismaleimide-glass or aromatic polyamide paper honeycomb cell structure filled or partially filled with a syntactic foam consisting of a mixture of bismaleimide resin and carbon microballoons.
The carbon microballoons are prepared by pyrolyzing phenolic microballoons and subsequently bonded using a 2% bismaleimide solution. The laminate structures are cured for two hours at 477.degree. K. and are adhered to the honeycomb bismaleimide adhesive using a pressure of 700 kN/m.sup.2 pressure at 450.degree. K. The laminate composite is then post-cured for two hours at 527.degree. K. to produce a composite laminate having a density in the range from about 95 kilograms per cubic meter to 130 kilograms per cubic meter.

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