Process for making .alpha.-chlorinated derivatives of 2-alkyl-2-

Details Process for making .alpha.-chlorinated derivatives of 2-alkyl-2- Process for making .alpha.-chlorinated derivatives of 2-alkyl-2-

1974-01-25

1976-06-08

Goldberg, Jerome D.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260307R, C07D26508, C07D27300, C07D29000

Patent

active

039622355

ABSTRACT:
The title compounds are prepared by contacting in liquid phase a 2-alkyl-2-oxazoline or oxazine with a t-alkyl hypochlorite. As an example, 2-chloromethyl-2-oxazoline was prepared in approximately 95 percent yield by contacting a substantially equimolar amount of 2-methyl-2-oxazoline with t-butyl hypochlorite for 19 hours at 23.degree.C in the dark. The process was conducted in carbon tetrachloride solution.

REFERENCES:
chem. Abst., 63, 13018(b), (1965),--Fell & Kung.
Chem. Abst., 65, 609(h), (1966)--Martin et al.
Chem. Abst., 66, 94933(u), (1967)--Aufderhaar et al.
The Merck Index, 7th Ed., --Merck & Co. Inc.--1960, p. 181.
Chem. Abst., 73, 45495(p) (1970)--Scherer et al.
Chem. Abst., 66, 94457(s), (1967)--Walling et al.

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