Distillation: apparatus – Apparatus – Systems
Patent
1978-02-27
1980-05-06
Yodkoff, Norman
Distillation: apparatus
Apparatus
Systems
203 87, 159DIG40, 417154, B01D 314, F04F 900
Patent
active
042016290
ABSTRACT:
A diffusion pump capable of separating impurities from its pump fluid during operation is disclosed. Skimming drains are provided in the pump's boiler for periodically skimming the evaporative surface of the working fluid. This eliminates nearly all contaminants of higher molecular weight than the pump fluid. In the foreline of the pump, a series of peripheral gutters are provided for trapping, separating and draining off condensates. The gutters facilitate the removal of impurities of lower molecular weight than that of the pump fluid. Means are also provided for further removing trace quantities of residual volatile impurities which tend to backstream up the diffusion pump barrel. The highly purified pump fluid allows for a more vigorously working evaporative surface, thereby increasing the throughput of the diffusion pump. Together with the elimination of volatile impurities from the pump barrel, this facilitates the attainment of significantly higher ultimate chamber vacuum. The withdrawn condensates and skimmed residues also form the basis for use of the apparatus as a device for obtaining a high degree of separation between liquids of very close vapor pressures.
REFERENCES:
patent: 2501276 (1950-03-01), Hickman
patent: 2752296 (1956-06-01), Lazare
patent: 3172922 (1965-03-01), Kehse
patent: 3496159 (1970-02-01), Spence
Barker, Jr. Vincent L.
Murray David D.
Yodkoff Norman
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