Purification of vitamin D.sub.3

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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26039725, C07J 900

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active

045295468

ABSTRACT:
Crude vitamin D.sub.3 is purified by reaction with a dienophile followed by short-path distillation.

REFERENCES:
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patent: 4388242 (1983-06-01), Malatesta et al.
The Vitamins, vol. III, 203, 1971.
Diels-Alder-Reaktion, H. Wollweber, Georg Thieme Verlag Stuttgart, 1972, pp. 54 to 65, 185-212.
H. Sauer, Angewandte Chemie, 1967, 79, p. 76.
The Application of Molecular Distillation, Hallo et al, Akademiai Kiado Budapest, 1971.

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